Synthesis of Hirsutene

C15H24
Principal investigator | Zhi-Xiang Yu |
---|---|
Publication year | 2008 |
Synthesis type | Total |
Number of steps | 8 (linear) |
References |
Part 1 of 1
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TBSOTf,
Et3N
Et2O
0 °C, 3 h, 100%


[Rh(CO)2Cl]2,
CO
1 atm.
Dioxane
80 °C, 48 h, 62%

ClCOCO2Me,
DMAP
CH2Cl2
RT, 1 h, 92%


