Part 1 of 1
intermediate structure
CaO
>180 °C, , 32%
intermediate structure
Na
EtOH
Reflux
intermediate structure
HI
H2O
RT to 100 °C, 3 h
intermediate structure
KOH
EtOH
Reflux, , 83% (3 steps)
intermediate structure
Br2
CHCl3
0 °C, , 100%
intermediate structure
Me2NH
PhH
140 °C, 5 h, 75%
intermediate structure
MeI
Acetone
RT
intermediate structure
Ag2O
H2O
RT to >120 °C, , 80%
intermediate structure
Br2
CHCl3
-5 °C, , 82%
intermediate structure
Quinoline
150-165 °C, , 94%
intermediate structure
HBr
AcOH
0 °C to RT, 2 h, 65%
intermediate structure
Me2NH
PhH
RT, 24 h, 92%
intermediate structure
Na
EtOH
Reflux, , 82%
intermediate structure
  1. Br2 , HBr
  2. Na2CO3
AcOH, H2O
intermediate structure
EtOH
Reflux, , 30% (2 steps)
intermediate structure
  1. NaOH
  2. KI
H2O
Reflux, 2 h
intermediate structure
AgCl
intermediate structure
130 °C, , 54% (3 steps)
intermediate structure
HBr
AcOH
100 °C, 80 h, 85%
intermediate structure
H2SO4
H2O
205-215 °C, 4 h, 24%
intermediate structure
CrO3
AcOH, H2O
60-70 °C, 4 h, 80%
intermediate structure
Na, CO2
Et2O
RT to reflux, 2 h, 82%
intermediate structure
HCl, Na(Hg)
H2O
10-12%
intermediate structure
HCl
MeOH
RT, 1 h
"No yield reported."
intermediate structure
Bz2O
PhH
Reflux
"No yield reported."
intermediate structure