Synthesis of [4,5]Coronane

Structure of [4,5]Coronane

C16H24

Principal investigatorLutz Fitjer
Publication year1987
Synthesis typeTotal
Number of steps 5 (linear)
References
Part 1 of 1
intermediate structure + intermediate structure
Et3N
80 °C to 120 °C, 5 h, 54%
intermediate structure
Special reagent
t-BuLi
Et2O
-78 °C, 3 h, 98%
intermediate structure
Al2O3, AgBF4
CCl4
-20 °C, 21 h, 52%
intermediate structure
Nafion-H
PhH
80 °C, 10 h, 100%
intermediate structure
Cyclohexane
RT, 14 h, 40%
intermediate structure