Synthesis of Hirsutene

Structure of Hirsutene

C15H24

Principal investigator	Andrew E. Greene
Publication year	1990
Synthesis type	Formal
Number of steps	6 (linear)
References	J. Am. Chem. Soc. 1990, 112, 9388.

Part 1 of 1

intermediate structure

+

intermediate structure

CuCN, ZnCl2, Mg

57%

intermediate structure

LiAlH4

74%

intermediate structure

Co2(CO)8

55%

See the Pauson-Khand Reaction

intermediate structure

Li

NH3

80%

intermediate structure

SmI2

85%

intermediate structure

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Remaining...

2.0% (11 steps)

"See: Tetrahedron Lett. 1976, 17, 195."

intermediate structure