Synthesis of Hirsutene
C15H24
| Principal investigator | Paul A. Wender |
|---|---|
| Publication year | 1982 |
| Synthesis type | Total |
| Number of steps | 8 (linear) |
| References |
Part 1 of 1
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hν
Cyclohexane
LiAlH4
Et2O
22-23% (2 steps)
Camphorsulfonic acid
PhH
RT, 71%
PhSH
100 °C, 78%
H2
CH2Cl2
"No yield reported. Several cycling were need to fully convert this product."
NaIO4
MeOH
86%
P(OMe)3
PhH
170 °C, 60%