Synthesis of Hirsutene
C15H24
| Principal investigator | Andrew E. Greene |
|---|---|
| Publication year | 1980 |
| Synthesis type | Formal |
| Number of steps | 10 (linear) |
| References |
Part 1 of 1
+
+
+
Et3N
NaBH4
100%
Cr(ClO4)2
50-60%
+
Zn-Cu,
POCl3
Et2O
60%
NaBH4
Cr(ClO4)2
HCO2H,
HClO4
H2O
Remaining...
70% (1 step)
"See: <i>Tetrahedron Lett. 1976, 17, 195."