Synthesis of Hirsutene

C15H24
Principal investigator | Shigeo Nozoe |
---|---|
Publication year | 1976 |
Synthesis type | Total |
Number of steps | 11 (linear) |
References |
Part 1 of 1

NaH,
AllylCl
DME
71%



Pyr,
OsO4
Et2O
-78 °C

NaIO4
H2O, THF
50% (2 steps)


Pyr,
(COCl)2
PhH

SnCl4
CS2
30 °C, 20% (2 steps)

Li
Et2O, NH3, t-BuOH


