Synthesis of Cubane

C8H8
Principal investigator | John Tsanaktsidis |
---|---|
Publication year | 1997 |
Synthesis type | Total |
Number of steps | 10 (linear) |
References |
Part 1 of 1

(CH2OH)2,
Dowex 50WX8
Dean-Stark
PhH
Reflux, 30 h, 90%

Br2
Dioxane
RT, 2 d


H2SO4
RT, 30.5 h, 92%

HCl
hν
H2O, MeOH
RT



NaOH
H2O, MeOH
Reflux, 4 h, 99%

SOCl2
Reflux, 2 h

