Synthesis of Panacene

C15H15BrO2
Principal investigator | Ken S. Feldman |
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Publication year | 1982 |
Synthesis type | Total |
Number of steps | 13 (linear) |
References |
Part 1 of 1
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AllylBr,
NaH
DMF

HCl
MeOH

K(s-Bu)3BH
THF
63% (3 steps)

NBS
MeCN

KOAc
DMF

NaOMe
MeOH



THF

n-Bu4N+ F-
THF
15% (2 steps)
"Also isolated was the epimer (10 % yield)."

MsCl,
Et3N
CH2Cl2

LiCuBr2
THF
69% (2 steps)
