Synthesis of Prismane

C6H6
Principal investigator | Thomas J. Katz |
---|---|
Publication year | 1973 |
Synthesis type | Total |
Number of steps | 5 (linear) |
References |
Part 1 of 1
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MeLi,
CH2Cl2
Et2O
-45 °C, 45%


Dioxane , Et2O
0 °C to RT, 60 min, 50-60%

KOH
H2O, MeOH
Reflux, 24 h

HCl,
CuCl2
H2O
65% (2 steps)

hν
PhMe
30 °C, 5 h, 8%
