N-(4-Methoxybenzyl)indole (PMB)
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Protection :
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ReagentsTimeYield
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NaH (4-MeOPh)CH2Cl35 min94 %NaH, (4-MeOPh)CH2ClDMF0 °C to RT, 35 min, 94%
Deprotection :
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ReagentsTimeYield
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PhSH13 h66 %PhSHCF3CO2H45 °C, 13 h, 66%