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Named Reactions
Protecting Groups
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Named Reactions
Protecting Groups
Formamide
Protection :
Reagents
Solvents
Temperature
Time
Yield
Et3N
HCO2Et
N/A
Reflux
ON
92 %
info
HCO2Et
Et3N
Reflux, ON, 92%
HCO2Ph
EtOAc
Reflux
45 min
94 %
info
HCO2Ph
EtOAc
Reflux, 45 min, 94%
HCO2Ac
HCO2H
RT - 50 °C
30 min - 12 h
90 - 95 %
info
HCO2Ac
HCO2H
RT to 50 °C, 30 min, 95%
info
HCO2Ac
HCO2H
RT, 12 h, 90%
Deprotection :
Reagents
Solvents
Temperature
Time
Yield
HCl
H2O
MeOH
Reflux
18 h
98 %
info
HCl
H2O
,
MeOH
Reflux, 18 h, 98%
HCl
Acetone
H2O
Reflux
60 min
79 %
info
HCl
Acetone
,
H2O
Reflux, 60 min, 79%
NaOH
MeOH
RT
20 h
80 %
info
NaOH
MeOH
RT, 20 h, 80%