Synthesis of Panacene
C15H15BrO2
Principal investigator | Ken S. Feldman |
---|---|
Publication year | 1982 |
Synthesis type | Total |
Number of steps | 13 (linear) |
References |
Part 1 of 1
+
+
AllylBr,
NaH
DMF
HCl
MeOH
K(s-Bu)3BH
THF
63% (3 steps)
NBS
MeCN
KOAc
DMF
NaOMe
MeOH
THF
n-Bu4N+ F-
THF
15% (2 steps)
"Also isolated was the epimer (10 % yield)."
MsCl,
Et3N
CH2Cl2
LiCuBr2
THF
69% (2 steps)