4-Methoxybenzenesulfonamide

4-Methoxybenzenesulfonamide scheme

Protection :

  • Reagents
    Solvents
    Temperature
    Time
    Yield
  • DMAP i-Pr2NEt 4-Methoxybenzenesulfonyl chloride
    CH2Cl2
    0 °C - RT
    24 h
    81 %
    info
    intermediate structure
    DMAP, i-Pr2NEt, 4-Methoxybenzenesulfonyl chloride
    CH2Cl2
    0 °C to RT, 24 h, 81%
    intermediate structure

Deprotection :

  • Reagents
    Solvents
    Temperature
    Time
    Yield
  • Na.Anthracene
    DME
    -30 °C - RT
    13.5 h
    90 %
    info
    intermediate structure
    Na.Anthracene
    DME
    -30 °C to RT, 13.5 h, 90%
    intermediate structure