Browse by molecules
Browse by principal investigator
Browse by date
Browse by carbon count
menu
Browse Syntheses
arrow_drop_down
Named Reactions
Protecting Groups
Browse Syntheses
arrow_drop_down
Browse by molecules
Browse by principal investigator
Browse by date
Browse by carbon count
Named Reactions
Protecting Groups
1-Chloroethyl carbamate (ACE)
Protection :
Reagents
Solvents
Temperature
Time
Yield
ClCO2CH(Cl)CH3
N/A
135 °C
2 d
72%
info
ClCO2CH(Cl)CH3
135 °C, 2 d, 72%
ClCO2CH(Cl)CH3
Proton Sponge
DCE
0 °C to refl
3.5 h
100%
info
ClCO2CH(Cl)CH3
,
Proton Sponge
DCE
0 °C to Reflux, 3.5 h, 100%
Deprotection :
Reagents
Solvents
Temperature
Time
Yield
N/A
MeOH
Reflux
3 h
100%
info
MeOH
Reflux, 3 h, 100%
info
MeOH
Reflux, 3 h, 100%