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Protecting Groups
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Named Reactions
Protecting Groups
Vilsmeier-Haack Formylation
Mechanism of the Vilsmeier-Haack Formylation
Original publication
Ber. Dtsch. Chem. Ges.. 1927, 60, 119.
Reviews
Comp. Org. Syn.. 1991, 2, 777.
J. Prakt. Chem.. 1996, 338, 392.
Org. React.. 1997, 49, 1.
Sample reactions
info
POCl3
DMF
0 to 95 °C, 2.5 h, 90-96%
info
POCl3
DMF
-30 °C, 20 min, 89%
info
POCl3
,
DMF
DCE
-10 °C to RT, 40 min, 71%
info
POCl3
DMF
0 to 35 °C, 60 min, 99%
info
POCl3
DMF
RT, 24 h, 90%