Sample reactions
intermediate structure
KI
DMF
125 °C, , 70% (2 steps)
intermediate structure
intermediate structure
LiCl
DMSO, H2O
170 °C, 70 min, 83%
intermediate structure
intermediate structure
LiCl
DMSO, H2O
140 °C, 15 min, 71% (4 steps)
intermediate structure
intermediate structure
LiI.3H2O
DMF
Reflux, 18 h, 85%
intermediate structure
intermediate structure
LiI
DMF
Reflux, 2 h, 65% (2 steps)
intermediate structure
intermediate structure
LiI, 2,4,6-Collidine
80 °C, 60 min
intermediate structure
intermediate structure
LiCl
DMSO, H2O
140 °C, 17 h, 97% (2 steps)
intermediate structure
intermediate structure
LiCl
DMF
135 °C, 4 h, 88% (2 steps)
intermediate structure
intermediate structure
LiCl, Et3N.HCl
DMA
130 °C, 2.5 h, 84%
intermediate structure
intermediate structure
NaCl
DMF, H2O
Reflux, 35 h, 69%
intermediate structure
intermediate structure
NaCl
DMF, H2O
Reflux, 35 h, 67% (2 steps)
intermediate structure
intermediate structure
NaCl
DMF, H2O
Reflux, 4 h, 56%
intermediate structure
intermediate structure
LiCl
DMSO, H2O
160 °C, 2 h, 85%
intermediate structure