Sample reactions
intermediate structure
CBS Reagent
THF
RT, 6 h, 88%
intermediate structure
intermediate structure
CBS Reagent
CH2Cl2, PhMe
-78 °C, 5.5 d, 84%
intermediate structure
intermediate structure
CBS Reagent, Catecholborane
CH2Cl2
-78 °C, 10 h, 94%
intermediate structure
intermediate structure
CBS Reagent, Catecholborane
93%
intermediate structure
intermediate structure
CBS Reagent, BH3.Me2S
THF
-30 °C, 10 min, 75%
">99:01 e.r."
intermediate structure